8-(2,5-Dimethoxy-tetrahydro-2-furyl)-octanoic acid methyl ester → 9-Keto-12-oxo-dodecanoic acid, methyl ester

HRID 436525Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 436525
[CH3:1][O:2][C:3](=[O:20])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][C:11]1(OC)[CH2:15][CH2:14][CH:13]([O:16]C)[O:12]1>Cl>[CH3:1][O:2][C:3](=[O:20])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][C:11](=[O:12])[CH2:15][CH2:14][CH:13]=[O:16]

Komponenten

3

Edukt 1

HCID 541867608-(2,5-Dimethoxy-tetrahydro-2-furyl)-octanoic acid methyl ester

Produkt 1

HCID 150938019-Keto-12-oxo-dodecanoic acid, methyl ester

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 313Hydrochloric AcidLösungsmittel

Versuchsvorschrift

10.0 g of the compound of step B was stirred for 30 minutes with 2100 ml of 1N hydrochloric acid at room temperature. The mixture was then extracted rapidly several times with ether.

Aufarbeitung

  1. extractionThe mixture was then extracted rapidly several times with ether

Quellen und Nachweise

ORD-Eintrag
ord-24b6c66e261f407fa89e024bb3d022c9
Quelldatensatz
uspto-grants-1977_02
Patentnummer
US04009187

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