HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Cystamine Dihydrochloride → HCID 21453017, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Cystamine Dihydrochloride | HCID 5941 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | 4-(Trifluoromethoxy)benzoyl Chloride | HCID 142110 | — |
| Lösungsmittel | 1,2-Dichloroethane | HCID 11 | — |
| Produkt | HCID 21453017 | HCID 21453017 | — |
Reaktionsschritte
m.p. 150°-151° C., 14.5 g., was prepared as in Example 1 using 33.6 g. of 4-trifluoromethoxybenzoyl chloride in 100 ml. of ethylene dichloride, 11.3 g. of cystamine dihydrochloride, 300 ml. of 10% sodium hydroxide solution, 400 ml. of ethylene dichloride and recrystallization from acetonitrile using decolorizing charcoal.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04009208 |
| Quelldatensatz | uspto-grants-1977_02 |
| ORD ID | ord-6f459ac2cfe64807a84e0880839d34fc |
| Quellennotiz | uspto-grants-1977_02 |