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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 436649Erstellt: 23. Oktober 2026

Cystamine Dihydrochloride → HCID 21453017, Verbindung

https://huagongshe.com/de/reaction/436649

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktCystamine DihydrochlorideHCID 5941—
EduktSodium HydroxideHCID 14798—
Edukt4-(Trifluoromethoxy)benzoyl ChlorideHCID 142110—
Lösungsmittel1,2-DichloroethaneHCID 11—
ProduktHCID 21453017HCID 21453017—

Reaktionsschritte

m.p. 150°-151° C., 14.5 g., was prepared as in Example 1 using 33.6 g. of 4-trifluoromethoxybenzoyl chloride in 100 ml. of ethylene dichloride, 11.3 g. of cystamine dihydrochloride, 300 ml. of 10% sodium hydroxide solution, 400 ml. of ethylene dichloride and recrystallization from acetonitrile using decolorizing charcoal.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04009208
Quelldatensatzuspto-grants-1977_02
ORD IDord-6f459ac2cfe64807a84e0880839d34fc
Quellennotizuspto-grants-1977_02