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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 436655Erstellt: 24. Oktober 2026

Potassium Hydroxide → N,N'-Dodecamethylenebis(4-trifluoromethoxybenzamide)

https://huagongshe.com/de/reaction/436655

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPotassium HydroxideHCID 14797—
Edukt1,12-DodecanediamineHCID 17727—
Edukt4-(Trifluoromethoxy)benzoyl ChlorideHCID 142110—
Lösungsmittel1,2-DichloroethaneHCID 11—
ProduktN,N'-Dodecamethylenebis(4-trifluoromethoxybenzamide)HCID 21452860—

Reaktionsschritte

m.p. 158°-159° C., 11.3 g., was prepared as in Example 1 using 24.8 g. of 4-trifluoromethoxybenzoyl chloride in 150 ml. of ethylene dichloride, 10.0 g. of 1,12-dodecanediamine, 60 ml. of 10% aqueous potassium hydroxide solution, 350 ml. of ethylene dichloride and recrystallization twice from ethanol and once from isopropyl alcohol.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04009208
Quelldatensatzuspto-grants-1977_02
ORD IDord-dcc3d143b4c94612acec4c4e25b57104
Quellennotizuspto-grants-1977_02