N,N-Dimethylallylamine → Allyl n-butoxymethyl dimethylammonium chloride

HRID 437030

Reaktionsgleichung

Reaktionsgleichung von HRID 437030
[CH2:1]([O:5][CH2:6][Cl:7])[CH2:2][CH2:3][CH3:4].[CH2:8]([N:11]([CH3:13])[CH3:12])[CH:9]=[CH2:10]>C(OCC)(=O)C>[Cl-:7].[CH2:8]([N+:11]([CH2:6][O:5][CH2:1][CH2:2][CH2:3][CH3:4])([CH3:13])[CH3:12])[CH:9]=[CH2:10]

Komponenten

4

Edukt 2

HCID 75082N,N-DimethylallylamineHCID 111053571-(Chloromethoxy)butane

Produkt 1

HCID 21429949Allyl n-butoxymethyl dimethylammonium chloride

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 8857Ethyl AcetateLösungsmittel

Versuchsvorschrift

24.7 grams of chloromethyl butyl ether was added to 17 grams of allyl dimethylamine in 32 grams of ethyl acetate. The reaction was highly exothermic and two layers formed very rapidly. Stirring was continued at 25° C. for 24 hours, after which the solvent was removed by vacuum. Chloride analysis of the rather viscous liquid product indicated 91% of theoretical.

Aufarbeitung

  1. customtwo layers formed very rapidly
  2. customafter which the solvent was removed by vacuum

Quellen und Nachweise

ORD-Eintrag
ord-555e2f750b504c65a2b53b679bcae8c9
Quelldatensatz
uspto-grants-1977_06
Patentnummer
US04029658

Verknüpfte Notizen

Wird geladen…