1-Methylpiperazine → HCID 53865690, Verbindung
Reaktionsgleichung
Cl[C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][C:3]=1[S:11]([N:14]([CH:16]1[CH2:21][CH2:20][CH2:19][CH2:18][CH2:17]1)[CH3:15])(=[O:13])=[O:12].[CH3:22][N:23]1[CH2:28][CH2:27][NH:26][CH2:25][CH2:24]1>>[CH3:15][N:14]([CH:16]1[CH2:21][CH2:20][CH2:19][CH2:18][CH2:17]1)[S:11]([C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][C:2]=1[N:26]1[CH2:27][CH2:28][N:23]([CH3:22])[CH2:24][CH2:25]1)[C:6]([OH:8])=[O:7])(=[O:13])=[O:12]Komponenten
3
Versuchsvorschrift
The reaction was carried out in a manner analogous to that of Example 31, using 33 g of 4-chloro-3-(N-methylcyclohexylaminosulfonyl)-benzoic acid and 30 g of N-methylpiperazine. The moist crude product, which had been washed with water, was freed from by-products by boiling with methanol.
Aufarbeitung
- washThe moist crude product, which had been washed with water
Quellen und Nachweise
- ORD-Eintrag
- ord-09156b18fbd34cb9948e0ef9cfd9d4b5