HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5-Bromovanillin → N-(3-chlorophenyl)-2-cyano-3-(3-bromo-4-hydroxy-5-methoxyphenyl) propenamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5-Bromovanillin | HCID 18099 | — |
| Edukt | N-(3-chlorophenyl)-2-cyanoacetamide | HCID 679494 | — |
| Produkt | N-(3-chlorophenyl)-2-cyano-3-(3-bromo-4-hydroxy-5-methoxyphenyl) propenamide | HCID 53730904 | 65% |
Reaktionsschritte
The reaction was performed in the same manner as in Example 1 with 5-bromovanillin (1.38 g, 5.97 mmol) and N-(3-chlorophenyl) cyanoacetamide (1.16 g, 5.97 mmol) to give the objective N-(3-chlorophenyl)-2-cyano-3-(3-bromo-4-hydroxy-5-methoxyphenyl) propenamide (1.58 g, 65% in yield).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05514711 |
| Quelldatensatz | uspto-grants-1996_05 |
| ORD ID | ord-4408703937e1495ea883d675cacea422 |
| Quellennotiz | uspto-grants-1996_05 |