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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 439758Erstellt: 24. Oktober 2026

N-heptylacetamide → 1-Heptanamine, N-ethyl-

https://huagongshe.com/de/reaction/439758

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktN-heptylacetamideHCID 347488—
EduktAluminium lithium hydrideHCID 21226445—
EduktSodium hydroxide--water (1/1/1)HCID 23719242—
LösungsmittelDiethyl EtherHCID 3283—
Produkt1-Heptanamine, N-ethyl-HCID 48038—

Reaktionsschritte

A mixture of a solution of 5.5 gms of the N-heptylacetamide in 150 ml of diethyl ether and 3.99 gms of lithium aluminum hydride are stirred at room temperature for 18 hours. The reaction mixture is then worked up with H2O/NaOH by the Fieser method, following which the organic layer is dried over MgSO4, filtered, and concentrated under vacuum to give N-heptyl-N-ethylamine.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05516767
Quelldatensatzuspto-grants-1996_05
ORD IDord-f49d0bbef8994d8586fdec05440b8c94
Quellennotizuspto-grants-1996_05