HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethanol → HCID 86749507, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethanol | HCID 702 | — |
| Edukt | 2-Ethylhexylamine | HCID 7719 | — |
| Edukt | Sodium Acetate | HCID 517045 | — |
| Edukt | 2-(4-Camphylidenemethylene-anilino)-4,6-dichloro-1,3,5-triazine | HCID 86749508 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | HCID 86749507 | HCID 86749507 | — |
Reaktionsschritte
A reaction mixture comprising 33 g (0.26 mol) of 2-ethylhexylamine and 50 g (0.12 mol) of 2-(4-camphylidenemethylene-anilino)-4,6-dichloro-1,3,5-triazine in toluene is heated to 90° C. in the presence of sodium acetate. When the starting materials have reacted completely, the mixture is worked up. The product (95%) is a yellow viscous oil. UV (ethanol, c=1 mg/100 ml): λmax =345 nm, E=0.57.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05520906 |
| Quelldatensatz | uspto-grants-1996_05 |
| ORD ID | ord-421b47c7408749a68881a84dac61fe1d |
| Quellennotiz | uspto-grants-1996_05 |