Sodium Bicarbonate → HCID 86626532, Verbindung

HRID 44156Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 44156
[C:1]([O:8][CH:9]1[CH:14]([CH:15]([CH3:17])[CH3:16])[CH2:13][CH2:12][CH:11]([CH3:18])[CH2:10]1)(=[O:7])[CH2:2][CH2:3][C:4]([O-:6])=[O:5].C(=O)(O)[O-].[Na+:23]>C(O)C>[C:1]([O:8][CH:9]1[CH:14]([CH:15]([CH3:17])[CH3:16])[CH2:13][CH2:12][CH:11]([CH3:18])[CH2:10]1)(=[O:7])[CH2:2][CH2:3][C:4]([O-:6])=[O:5].[Na+:23]

Komponenten

4

Edukt 2

HCID 516892Sodium BicarbonateHCID 186766644-{[5-Methyl-2-(propan-2-yl)cyclohexyl]oxy}-4-oxobutanoate2×

Produkt 1

HCID 86626532HCID 86626532, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

Monomenthyl succinate (0.5 g, 1.95 mmol) was dissolved in ethanol (6.3 ml). Sodium bicarbonate solution (0.196 g, 2.33 mmol in 10 ml DI H2O) was slowly added to the monomenthyl succinate solution at room temperature. The mixture was stirred for 19 hours. Water and ethanol were removed by rotary evaporator at 50° C., followed by high vacuum line at 50° C. to give sodium monomenthyl succinate as a fine white powder.

Aufarbeitung

  1. customWater and ethanol were removed by rotary evaporator at 50° C.
  2. customfollowed by high vacuum line at 50° C.

Quellen und Nachweise

ORD-Eintrag
ord-2797674f93f64de495e77f069694f599
Quelldatensatz
uspto-grants-2013_09
Patentnummer
US08541401B2

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