Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 441760Erstellt: 25. Oktober 2026

Acetylacetone → 2,8-Dimethyldibenzofuran

https://huagongshe.com/reaction/441760

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAcetylacetoneHCID 31261—
EduktBenzene, 1,1'-oxybis[4-methyl-HCID 74098—
Katalysatorpalladium(II) acetateHCID 167845—
Produkt2,8-DimethyldibenzofuranHCID 63931920,6%

Reaktionsschritte

This example was carried out under the same reaction conditions as in Example 1 except that 29.0 g of 4,4'-dimethyldiphenyl ether, 0.067 g (0.30 m. mole) of palladium acetate, and 0.030 g of acetylacetone (0.30 m. mole) were employed and the mixture was reacted for 7 hours. As a result, 5.9 g (30 m. moles) of 2,8 -dimethyldibenzofuran was obtained and 1.9 g (4.7 m. moles) of the dimer also obtained.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04042603
Quelldatensatzuspto-grants-1977_08
ORD IDord-1c4aa2f80db2461c8e90f3be876f0c41
Quellennotizuspto-grants-1977_08