HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Oxygen → Diphenylformamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Oxygen | HCID 977 | — |
| Edukt | Methyldiphenylamine | HCID 11098 | — |
| Produkt | Diphenylformamide | HCID 69081 | 43,3% |
Reaktionsschritte
By essentially the procedure of Example 1, a tube was charged with 40 g of methyldiphenylamine and 2.0 g CuCl2. 2H2O. The reaction was run at 115°-125° C. for 2 hr at 290-400 psi. About 0.1 mole of oxygen was injected incrementally. GC/MS analysis showed a 98.6% conversion of methyldiphenylamine and a 43.3% yield of diphenylformamide.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04042621 |
| Quelldatensatz | uspto-grants-1977_08 |
| ORD ID | ord-9030a9fdf81e4b68b1daa6a663d70bb7 |
| Quellennotiz | uspto-grants-1977_08 |