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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 441808Erstellt: 23. Oktober 2026

Benzyl Bromide → 2-Benzyl-6-methoxyisoquinolinium bromide

https://huagongshe.com/de/reaction/441808

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBenzyl BromideHCID 7498—
Edukt6-MethoxyisoquinolineHCID 11040978—
LösungsmittelAcetoneHCID 180—
LösungsmittelDiethyl EtherHCID 3283—
Produkt2-Benzyl-6-methoxyisoquinolinium bromideHCID 21418213—

Reaktionsschritte

6-Methoxyisoquinoline (1.6 g) and benzyl bromide (2 ml) in acetone (75 ml) were heated under reflux for 1 hour. The mixture was diluted with ether and cooled to 0°. The solid was filtered off and recrystallised from methanol/ether, and had m.p. 155°-158°.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04042697
Quelldatensatzuspto-grants-1977_08
ORD IDord-a515023c47354e99bfa7c2376c17c423
Quellennotizuspto-grants-1977_08