HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetic Acid → 2-nitroethyl Acetate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetic Acid | HCID 176 | — |
| Edukt | Benzene | HCID 241 | — |
| Edukt | HCID 22056827 | HCID 22056827 | — |
| Katalysator | Sulfuric Acid | HCID 1118 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 2-nitroethyl Acetate | HCID 11815399 | — |
Reaktionsschritte
64 g nitroethanol, 50 ml glacial acetic acid, 250 ml benzene and 5 drops conc. H2SO4 were refluxed, using a water separator for 8 hours; 12 ml of H2O were collected. The solution was evaporated and vacuum distilled (1mm at 60° C) yielding 89 g colorless nitroethylacetate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04044020 |
| Quelldatensatz | uspto-grants-1977_08 |
| ORD ID | ord-69984e74caad4c0abca1aeb28fb2ec24 |
| Quellennotiz | uspto-grants-1977_08 |