Acetic Acid → 2-nitroethyl Acetate

HRID 442021

Reaktionsgleichung

Reaktionsgleichung von HRID 442021
[N+:1]([CH:4](O)[CH3:5])([O-:3])=[O:2].[C:7]([OH:10])(=[O:9])[CH3:8].C1C=CC=CC=1>OS(O)(=O)=O.O>[N+:1]([CH2:4][CH2:5][O:10][C:7](=[O:9])[CH3:8])([O-:3])=[O:2]

Komponenten

6

Edukt 3

HCID 176Acetic AcidHCID 241BenzeneHCID 22056827HCID 22056827, Verbindung

Produkt 1

HCID 118153992-nitroethyl Acetate

Reagenzien, Katalysatoren, Lösungsmittel 2

HCID 1118Sulfuric AcidKatalysatorHCID 962WaterLösungsmittel

Versuchsvorschrift

64 g nitroethanol, 50 ml glacial acetic acid, 250 ml benzene and 5 drops conc. H2SO4 were refluxed, using a water separator for 8 hours; 12 ml of H2O were collected. The solution was evaporated and vacuum distilled (1mm at 60° C) yielding 89 g colorless nitroethylacetate.

Aufarbeitung

  1. customfor 8 hours
  2. custom12 ml of H2O were collected
  3. customThe solution was evaporated
  4. distillationvacuum distilled (1mm at 60° C)

Quellen und Nachweise

ORD-Eintrag
ord-69984e74caad4c0abca1aeb28fb2ec24
Quelldatensatz
uspto-grants-1977_08
Patentnummer
US04044020

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