HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Phenyl phenylglyoxylate → Phenyl 4-chlorobenzoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Phenyl phenylglyoxylate | HCID 13975017 | — |
| Edukt | 4-Chlorophenyl phenylglyoxylate | HCID 54442020 | — |
| Katalysator | Tetraphenylphosphonium Chloride | HCID 164911 | — |
| Lösungsmittel | Chloroform | HCID 6212 | — |
| Produkt | Phenyl 4-chlorobenzoate | HCID 260766 | — |
Reaktionsschritte
The decarbonylation reaction of Example 79 was repeated except that phenyl phenylglyoxylate (PPG) was replaced with 4-chlorophenyl phenylglyoxylate (4-CPPG), and that the amounts of tetraphenylphosphonium chloride and chloroform were changed as set forth in Table 13. The results are set forth in Table 13.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05892091 |
| Quelldatensatz | uspto-grants-1999_04 |
| ORD ID | ord-b4c01714edc043b29f69990524dc94d0 |
| Quellennotiz | uspto-grants-1999_04 |