Reaktionsgleichung
[CH:1]1[CH:6]=[C:5]2[C:7]([NH:9][C:10]3=[CH:11][CH:12]=[CH:13][C:3](=[C:4]23)[CH:2]=1)=O.C1(CC#N)C(C[C:21]#[N:22])=CC=CC=1.C(C=O)=O.[OH-].[Na+].[OH-].[K+]>>[C:21]([C:2]1[C:3]2[C:4](=[CH:10][CH:11]=[CH:12][CH:13]=2)[C:5]([C:7]#[N:9])=[CH:6][CH:1]=1)#[N:22]Komponenten
6
Versuchsvorschrift
The naphtholactam compounds of the formula (II) used as starting products are obtainable by reacting o-xylylenedicyanide with glyoxal in the presence of a base (NaOH, KOH) and of a solvent at temperatures below 50° C. (e.g. 0° to 40° C.) to give 1,4-dicyanonaphthalene, and subsequently either
Quellen und Nachweise
- ORD-Eintrag
- ord-6009ed9f7ab64d34978729b15188251f
- Quelldatensatz
- uspto-grants-1981_04
- Patentnummer
- US04260770
Verknüpfte Notizen
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