HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dichloromethane → 2-(2-Naphthyloxy)ethyl methanesulfonate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dichloromethane | HCID 6344 | — |
| Edukt | 2-(2-Naphthoxy)ethanol | HCID 7131 | — |
| Edukt | Methanesulfonyl chloride | HCID 31297 | — |
| Lösungsmittel | Triethylamine | HCID 8471 | — |
| Produkt | 2-(2-Naphthyloxy)ethyl methanesulfonate | HCID 19004383 | — |
Reaktionsschritte
As described in Example 2, 13.5 g. of 2-(2-naphthyloxy)ethanol in 400 ml. of dichloromethane is reacted with 9.5 g. of methanesulfonyl chloride in the presence of 11.4 g. of triethylamine to give the product as tan crystals.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04260816 |
| Quelldatensatz | uspto-grants-1981_04 |
| ORD ID | ord-e0de3a90955d439684568c996684aa72 |
| Quellennotiz | uspto-grants-1981_04 |