Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Isoprene | HCID 6557 | — |
| Edukt | 1,3-Butadiene | HCID 7845 | — |
| Edukt | Butyllithium | HCID 178418339 | — |
| Lösungsmittel | Heptane | HCID 8900 | — |
| Produkt | Isoprene butadiene | HCID 168288 | — |
Reaktionsschritte
In a reactor, a mixture of 57 g of 1,3-butadiene and 37 g of isoprene is added to a solution of 12.5 mmoles of butyllithium in 250 ml of n-heptane. The reaction mixture is stirred for 5 hours at 50° C., which results in a complete conversion of the monomers to a butadiene-isoprene copolymer having a butadiene content of 60% by weight and an average molecular weight by number of 5700.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US04264334 |
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| Quelldatensatz | uspto-grants-1981_04 |
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| ORD ID | ord-daee73f20a3c41f9971fe910bad41998 |
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| Quellennotiz | uspto-grants-1981_04 |
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