Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Isobutyronitrile | HCID 6559 | — |
| Edukt | Fluorobenzene | HCID 10008 | — |
| Edukt | Potassium bis(trimethylsilyl)amide | HCID 3251421 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Lösungsmittel | Diethyl Ether | HCID 3283 | — |
| Produkt | 2-Methyl-2-phenylpropanenitrile | HCID 2797591 | 50,4% |
Reaktionsschritte
To a solution of fluorobenzene (5.85 mL, 62.4 mmol) in 100 mL of anhydrous toluene was added isobutyronitrile (22.5 mL, 250 mmol) followed by 200 mL (100 mmol) of a 0.5 M solution of KHMDS in toluene. The reaction was stirred at 80° C. for 24 hours. The reaction was then allowed to cool to room temperature, diluted with diethyl ether, and washed with water and brine. The organic fraction was dried over sodium sulfate and concentrated under reduced pressure. The product was purified by flash chromatography using an ethyl acetate/hexanes gradient to yield 4.57 g (50%) of the objective compound as a brown oil. MS: (ESI, Pos) m/z 168.0 (M+23). 1H NMR (500 MHz, CDCl3): δ (ppm) 7.48 (d, 2H), 7.39 (t, 2H), 7.31 (t, 1H), 1.73 (s, 6H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US08541431B2 |
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| Quelldatensatz | uspto-grants-2013_09 |
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| ORD ID | ord-0527e5fadd774f6898b206182be29928 |
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| Quellennotiz | uspto-grants-2013_09 |
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