1,12-Dodecanediamine → N-[1-(Methylamino)-2-nitroethenyl]-1,12-dodecanediamine

Beteiligte Stoffe

Reaktionsschritte

A mixture of 1,12-diaminododecane (3 g) and N-methyl-1-(methylthio)-2-nitroethenamine (1.48 g) in water (50 ml) was stirred at room temperature for 20 hours. The solution was evaporated in vacuo and the residue chomatographed (silica/methanol). The appropriate eluate was evaporated to yield the title compound (1.8 g), mp. 123°-125°.

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