HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
p-Chlorothiophenol → 2-[(4-Chlorophenyl)thio]benzonitrile
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | p-Chlorothiophenol | HCID 7815 | — |
| Edukt | 2-Chlorobenzonitrile | HCID 13391 | — |
| Edukt | 2-Chlorothioxanthone | HCID 618848 | — |
| Produkt | 2-[(4-Chlorophenyl)thio]benzonitrile | HCID 3018342 | — |
Reaktionsschritte
Method of preparing 2-chloro-thioxanthone which comprises reacting an alkali metal derivative of 4-chloro-thiophenol with 2-chloro-benzonitrile in an organic solvent to form 2-(4'-chloro-phenylthio)-benzonitrile, hydrolyzing said 2-(4'-chloro-phenylthio)-benzonitrile to form 2-(4'l -chloro-phenylthio)-benzoic acid and cyclising said 2-(4'-chloro-phenylthio)-benzoic acid by dehydration to produce 2-cloro-thioxanthone.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04264773 |
| Quelldatensatz | uspto-grants-1981_04 |
| ORD ID | ord-3492703b83774406951c0e57200566ac |
| Quellennotiz | uspto-grants-1981_04 |