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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 444602Erstellt: 27. Oktober 2026

p-Chlorothiophenol → 2-[(4-Chlorophenyl)thio]benzonitrile

https://huagongshe.com/reaction/444602

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Eduktp-ChlorothiophenolHCID 7815—
Edukt2-ChlorobenzonitrileHCID 13391—
Edukt2-ChlorothioxanthoneHCID 618848—
Produkt2-[(4-Chlorophenyl)thio]benzonitrileHCID 3018342—

Reaktionsschritte

Method of preparing 2-chloro-thioxanthone which comprises reacting an alkali metal derivative of 4-chloro-thiophenol with 2-chloro-benzonitrile in an organic solvent to form 2-(4'-chloro-phenylthio)-benzonitrile, hydrolyzing said 2-(4'-chloro-phenylthio)-benzonitrile to form 2-(4'l -chloro-phenylthio)-benzoic acid and cyclising said 2-(4'-chloro-phenylthio)-benzoic acid by dehydration to produce 2-cloro-thioxanthone.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04264773
Quelldatensatzuspto-grants-1981_04
ORD IDord-3492703b83774406951c0e57200566ac
Quellennotizuspto-grants-1981_04