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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 445764Erstellt: 24. Oktober 2026

Ethanol → 2-(5-Bromo-pyridin-3-yl)-N-methyl-acetamide

https://huagongshe.com/de/reaction/445764

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktEthanolHCID 702—
EduktMethylamineHCID 6329—
Edukt2-(5-Bromopyridin-3-yl)acetic acidHCID 2802539—
Produkt2-(5-Bromo-pyridin-3-yl)-N-methyl-acetamideHCID 54236812—

Reaktionsschritte

The title compound was synthesized in a similar manner as described for Example 103 using (5-bromo-pyridin-3-yl)-acetic acid (ABCR, Karlsruhe, Germany, 1.815 mmol) and 8 M methylamine in EtOH (Aldrich, Buchs, Switzerland, 7.26 mmol) to give the title compound as an off-white solid. (HPLC: tR 1.74 min (Method A); M+H=229, 231 MS-ES)

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08476294B2
Quelldatensatzuspto-grants-2013_07
ORD IDord-2a07b27fc62142d5a8c6f5ad95515fb3
Quellennotizuspto-grants-2013_07