Hydrochloric Acid → (6-Methylpyridin-2-yl)methanol hydrochloride

Beteiligte Stoffe

Reaktionsschritte

A solution of (6-methylpyridin-2-yl)methyl acetate (1.0 g) in concentrated HCl (3 mL) was refluxed for 1 h. The reaction mixture was then concentrated in vacuo to obtain the crude product. The crude material was azeotroped with toluene, and the residue obtained was filtered and dried in vacuo to afford (6-methylpyridin-2-yl)methanol hydrochloride (811 mg) as a solid.

Herkunft & Nachweise