HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
p-Toluenesulfonic acid → 2-p-Cyanophenyl-5-n-pentyl-4-methyl-1,3-dioxane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | p-Toluenesulfonic acid | HCID 6101 | — |
| Edukt | 4-Cyanobenzaldehyde | HCID 66042 | — |
| Edukt | 3-Hydroxymethyl-2-octanol | HCID 13526101 | — |
| Lösungsmittel | Benzene | HCID 241 | — |
| Produkt | 2-p-Cyanophenyl-5-n-pentyl-4-methyl-1,3-dioxane | HCID 20150974 | — |
Reaktionsschritte
A mixture of 0.1 mol of p-cyanobenzaldehyde, 0.1 mol of 3-hydroxymethyl-2-octanol, 200 ml of benzene and 150 mg of p-toluenesulfonic acid is boiled under a water separator until the reaction is complete. Usual working-up gives 2-p-cyanophenyl-5-n-pentyl-4-methyl-1,3-dioxane.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04726911 |
| Quelldatensatz | uspto-grants-1988_02 |
| ORD ID | ord-f338593bb42141e5a94468c5d011ca54 |
| Quellennotiz | uspto-grants-1988_02 |