HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thionyl Chloride → 2,6-Dichloro-4-iodobenzoyl chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | 2,6-Dichloro-4-iodobenzoic acid | HCID 51341877 | — |
| Produkt | 2,6-Dichloro-4-iodobenzoyl chloride | HCID 86648958 | 100% |
Reaktionsschritte
A solution of 2,6-dichloro-4-iodobenzoic acid (65 mg, 0.21 mmol) in SOCl2 (3 mL) was heated to reflux under nitrogen atmosphere overnight and then cooled to room temperature. The reaction was conentrated under reduced pressure to afford 2,6-dichloro-4-iodobenzoyl chloride (70 mg, 100% yield).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08486950B2 |
| Quelldatensatz | uspto-grants-2013_07 |
| ORD ID | ord-4d56422000ae457ca41ed97b75cb9c61 |
| Quellennotiz | uspto-grants-2013_07 |