Dimethyl Sulfate → N,N,N',N',N''-Pentamethylguanidine

HRID 452359

Reaktionsgleichung

Reaktionsgleichung von HRID 452359
[CH3:1][N:2]([CH3:8])[C:3](=[NH:7])[N:4]([CH3:6])[CH3:5].S(OC)(O[CH3:13])(=O)=O>CN(C=O)C>[CH3:1][N:2]([CH3:8])[C:3](=[N:7][CH3:13])[N:4]([CH3:6])[CH3:5]

Komponenten

4

Edukt 2

HCID 6497Dimethyl SulfateHCID 664601,1,3,3-Tetramethylguanidine

Produkt 1

HCID 139457N,N,N',N',N''-Pentamethylguanidine

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 6228DimethylformamideLösungsmittel

Versuchsvorschrift

Tetramethlguanidine functionalized perfluorinated polymers were further treated with dimethyl sulfate (DMS) in DMF at 90° C. for 24 hr. Pentamethylguanidine functionalized perfluorinated polymer was obtained. Guanidine functionalized perfluorinated polymers was further treated with 1 M NaOH followed by washing with water.

Quellen und Nachweise

ORD-Eintrag
ord-8ed9385d323b4c9f82d6bcd44532a8b4
Quelldatensatz
uspto-grants-2013_07
Patentnummer
US08492049B2

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