HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-(3-Fluorophenyl)propionic acid → Tert-butyl [4-[[2-[3-(3-fluorophenyl)propanoyl]hydrazino]carbonyl]-2-pyridyl]carbamate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-(3-Fluorophenyl)propionic acid | HCID 2737489 | — |
| Edukt | Tert-butyl [4-(hydrazinocarbonyl)-2-pyridyl]carbamate | HCID 86640026 | — |
| Produkt | Tert-butyl [4-[[2-[3-(3-fluorophenyl)propanoyl]hydrazino]carbonyl]-2-pyridyl]carbamate | HCID 86640025 | 60% |
Reaktionsschritte
In the same manner as in Reference Example 1 and using 3-(3-fluorophenyl)propionic acid instead of benzothiazole-6-carboxylic acid and tert-butyl[4-(hydrazinocarbonyl)-2-pyridyl]carbamate instead of tert-butyl carbazate, the title compound (yield 60%) was obtained as colorless crystals.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08492378B2 |
| Quelldatensatz | uspto-grants-2013_07 |
| ORD ID | ord-2c88286c69ad48efb8394d62cacbe8aa |
| Quellennotiz | uspto-grants-2013_07 |