HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Methyl-1H-pyrazole-4-boronic acid → HCID 58294593, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Methyl-1H-pyrazole-4-boronic acid | HCID 11263501 | — |
| Edukt | HCID 58294405 | HCID 58294405 | — |
| Produkt | HCID 58294593 | HCID 58294593 | 32% |
Reaktionsschritte
The title compound is prepared from trifluoro-methanesulfonic acid cis-1-(2,2,2-trifluoro-acetyl)-2,3,4,4a,9,9a-hexahydro-1H-indeno[2,1-b]pyridin-6-yl ester and 1-methyl-pyrazol-4-yl-boronic acid following a procedure analogous to that described in Step 2 of Intermediates 17 and 18. Yield: 32% of theory; LC (method 1): tR=3.88 min; Mass spectrum (ESI+): m/z=350 [M+H]+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08497281B2 |
| Quelldatensatz | uspto-grants-2013_07 |
| ORD ID | ord-15400d6a29f54e33aea919d0fe2d6b40 |
| Quellennotiz | uspto-grants-2013_07 |