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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 456055Erstellt: 26. Oktober 2026

Methylhydrazine → 1-Methyl-2-[(2,4,6-trifluorophenyl)methylidene]hydrazine

https://huagongshe.com/reaction/456055

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktMethylhydrazineHCID 6061—
Edukt2,4,6-TrifluorobenzaldehydeHCID 521845—
LösungsmittelEthanolHCID 702—
Produkt1-Methyl-2-[(2,4,6-trifluorophenyl)methylidene]hydrazineHCID 87133126—

Reaktionsschritte

A solution of 2,4,6-Trifluoro-benzaldehyde (3 g, 18.74 mmol) and methyl hydrazine (40% in water, 2.6 ml, 18.74 mmol) in 20 ml anhydrous ethanol was stirred at room temperature for 1 hour. Solvent was evaporated to give the title compound as a white solid which was used in the next step without purification (3.95 g, 100%). LCMS (method B): [MH]+=189, tR=2.16 min.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08497368B2
Quelldatensatzuspto-grants-2013_07
ORD IDord-2515e85ee0fa4aacb624cf868c14af67
Quellennotizuspto-grants-2013_07