HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methylhydrazine → 1-Methyl-2-[(2,4,6-trifluorophenyl)methylidene]hydrazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methylhydrazine | HCID 6061 | — |
| Edukt | 2,4,6-Trifluorobenzaldehyde | HCID 521845 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 1-Methyl-2-[(2,4,6-trifluorophenyl)methylidene]hydrazine | HCID 87133126 | — |
Reaktionsschritte
A solution of 2,4,6-Trifluoro-benzaldehyde (3 g, 18.74 mmol) and methyl hydrazine (40% in water, 2.6 ml, 18.74 mmol) in 20 ml anhydrous ethanol was stirred at room temperature for 1 hour. Solvent was evaporated to give the title compound as a white solid which was used in the next step without purification (3.95 g, 100%). LCMS (method B): [MH]+=189, tR=2.16 min.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08497368B2 |
| Quelldatensatz | uspto-grants-2013_07 |
| ORD ID | ord-2515e85ee0fa4aacb624cf868c14af67 |
| Quellennotiz | uspto-grants-2013_07 |