Methylparaben → N-[4-(Cyclobutylmethoxy)benzoyl]glycine
Reaktionsgleichung
[CH:1]1([CH2:4][CH2:5][O:6][C:7]2[CH:19]=[CH:18][C:10]([C:11]([NH:13][CH2:14][C:15]([OH:17])=[O:16])=[O:12])=[CH:9][CH:8]=2)[CH2:3][CH2:2]1.OC1C=CC(C(OC)=O)=CC=1.C1(CO)CCC1>>[CH:4]1([CH2:5][O:6][C:7]2[CH:8]=[CH:9][C:10]([C:11]([NH:13][CH2:14][C:15]([OH:17])=[O:16])=[O:12])=[CH:18][CH:19]=2)[CH2:2][CH2:3][CH2:1]1Komponenten
4
Versuchsvorschrift
The same reactions as in Example 9 (9a) and (9b) were conducted using methyl 4-hydroxybenzoate (3.81 g, 25.0 mmol) and cyclobutylmethanol (2.36 mL, 25.0 mmol) to give 6.41 g of the title compound (colorless oil, yield: 97%).
Quellen und Nachweise
- ORD-Eintrag
- ord-9e811cdf7234417eb92153be84b970ab
- Quelldatensatz
- uspto-grants-2013_07
- Patentnummer
- US08497397B2
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