2,4-Dihydroxybenzophenone → 3-{4-[3-(4-Benzoyl-3-hydroxy-phenoxy)-propoxy]-phenyl}-2-methoxy-propionic acid ethyl ester
Reaktionsgleichung
[CH2:1]([O:3][C:4](=[O:20])[C@@H:5]([O:18][CH3:19])[CH2:6][C:7]1[CH:12]=[CH:11][C:10]([O:13][CH2:14][CH2:15][CH2:16]Br)=[CH:9][CH:8]=1)[CH3:2].[OH:21][C:22]1[CH:35]=[C:34]([OH:36])[CH:33]=[CH:32][C:23]=1[C:24]([C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1)=[O:25]>>[CH2:1]([O:3][C:4](=[O:20])[CH:5]([O:18][CH3:19])[CH2:6][C:7]1[CH:12]=[CH:11][C:10]([O:13][CH2:14][CH2:15][CH2:16][O:36][C:34]2[CH:33]=[CH:32][C:23]([C:24](=[O:25])[C:26]3[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=3)=[C:22]([OH:21])[CH:35]=2)=[CH:9][CH:8]=1)[CH3:2]Komponenten
3
Versuchsvorschrift
A mixture of (2S)-3-[4-(3-Bromo-propoxy)-phenyl]-2-methoxy-propionic acid ethyl ester from Step A and 2,4-dihydroxybenzophenone were allowed to react under the Standard Procedure I to get to title compound.
Aufarbeitung
- customto react under the Standard Procedure I