HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → 3,4-bis-(4-methoxyphenyl)-5-ethyl-4H-1,2,4-triazole hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | Diisopropyl Ether | HCID 7914 | — |
| Edukt | 3,4-bis-(4-methoxyphenyl)-5-ethyl-4H-1,2,4-triazole | HCID 13054018 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 3,4-bis-(4-methoxyphenyl)-5-ethyl-4H-1,2,4-triazole hydrochloride | HCID 20151545 | — |
Reaktionsschritte
2.9 ml of a solution of 5.9N hydrogen chloride in ethanol were aded to a solution of 5 g of the product of Example 1 in 5 ml of ethanol and the mixture was stirred while adding isopropyl ether thereto. The mixture was stirred for 24 hours and was filtered. The product was empasted with isopropyl ether, filtered and dried under pressure to obtain 4.4 g of 3,4-bis-(4-methoxyphenyl)-5-ethyl-4H-1,2,4-triazole hydrochloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04727084 |
| Quelldatensatz | uspto-grants-1988_02 |
| ORD ID | ord-29c1287a74224764a2342d6da5b34f12 |
| Quellennotiz | uspto-grants-1988_02 |