HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(3-Bromo-4-chlorophenyl)methanol → 3-Bromo-4-chlorobenzaldehyde
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (3-Bromo-4-chlorophenyl)methanol | HCID 50998689 | — |
| Katalysator | Manganese dioxide | HCID 14801 | — |
| Lösungsmittel | Acetone | HCID 180 | — |
| Produkt | 3-Bromo-4-chlorobenzaldehyde | HCID 14049809 | 62,4% |
Reaktionsschritte
A solution of 3-bromo-4-chlorobenzyl alcohol (3.24 g, 14.6 mmol) in acetone (100 mL) was treated with MnO2 (16.2 g, 73 mmol) and the mixture stirred for 3 days then filtered over diatomaceous earth. The filtrate was concentrated under reduced pressure to afford 2.0 g of title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07196102B2 |
| Quelldatensatz | uspto-grants-2007_03 |
| ORD ID | ord-294ab56614fc44a6a54189571da03d8a |
| Quellennotiz | uspto-grants-2007_03 |