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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 460126Erstellt: 25. Oktober 2026

(3-Bromo-4-chlorophenyl)methanol → 3-Bromo-4-chlorobenzaldehyde

https://huagongshe.com/reaction/460126

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt(3-Bromo-4-chlorophenyl)methanolHCID 50998689—
KatalysatorManganese dioxideHCID 14801—
LösungsmittelAcetoneHCID 180—
Produkt3-Bromo-4-chlorobenzaldehydeHCID 1404980962,4%

Reaktionsschritte

A solution of 3-bromo-4-chlorobenzyl alcohol (3.24 g, 14.6 mmol) in acetone (100 mL) was treated with MnO2 (16.2 g, 73 mmol) and the mixture stirred for 3 days then filtered over diatomaceous earth. The filtrate was concentrated under reduced pressure to afford 2.0 g of title compound.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07196102B2
Quelldatensatzuspto-grants-2007_03
ORD IDord-294ab56614fc44a6a54189571da03d8a
Quellennotizuspto-grants-2007_03