HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Borohydride → 4-Methoxy-3-(4-methoxyphenyl)benzyl alcohol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Borohydride | HCID 28123 | — |
| Edukt | 6,4'-Dimethoxybiphenyl-3-carbaldehyde | HCID 22391191 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 4-Methoxy-3-(4-methoxyphenyl)benzyl alcohol | HCID 68841639 | 87,2% |
Reaktionsschritte
A solution of 4-methoxy-3-(4-methoxyphenyl)benzenecarboxaldehyde (1 g, 4.13 mmol) in methanol (12 mL) was treated with polymer-supported borohydride (10.3 mmol) and the mixture shaken for 16 hours. The resin was then filtered and the filtrate concentrated under reduced pressure to afford 0.88 g of title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07196102B2 |
| Quelldatensatz | uspto-grants-2007_03 |
| ORD ID | ord-a9f128eb66ba4a03a994df7c3c66eb4c |
| Quellennotiz | uspto-grants-2007_03 |