Ethyl 4-benzyloxy-1-(2-methylpropyl)indole-2-carboxylate → Ethyl 4-hydroxy-1-(2-methylpropyl)indole-2-carboxylate

HRID 460554Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 460554
C([O:8][C:9]1[CH:17]=[CH:16][CH:15]=[C:14]2[C:10]=1[CH:11]=[C:12]([C:22]([O:24][CH2:25][CH3:26])=[O:23])[N:13]2[CH2:18][CH:19]([CH3:21])[CH3:20])C1C=CC=CC=1>[C].[Pd]>[OH:8][C:9]1[CH:17]=[CH:16][CH:15]=[C:14]2[C:10]=1[CH:11]=[C:12]([C:22]([O:24][CH2:25][CH3:26])=[O:23])[N:13]2[CH2:18][CH:19]([CH3:21])[CH3:20]

Komponenten

3

Edukt 1

HCID 22729270Ethyl 4-benzyloxy-1-(2-methylpropyl)indole-2-carboxylate

Produkt 1

HCID 22728995Ethyl 4-hydroxy-1-(2-methylpropyl)indole-2-carboxylate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 178418390HCID 178418390, VerbindungKatalysator

Versuchsvorschrift

By the reactions in the same manner as in Starting Material Synthesis Example 10 using ethyl 4-benzyloxy-1-(2-methylpropyl)indole-2-carboxylate (6.0 g) and 10% palladium-carbon (0.6 g), the title compound was obtained as pale-brown crystals.

Quellen und Nachweise

ORD-Eintrag
ord-691c4157271f4b1dac18465abd4e25d4
Quelldatensatz
uspto-grants-2007_03
Patentnummer
US07196199B2

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