N,N'-Dibutylthiourea → 3-n-Butyl-2-n-butylimino-4-(4-chloro-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrobromide
Reaktionsgleichung
[Br:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=1)=[O:4].[CH2:16]([NH:20][C:21]([NH:23][CH2:24][CH2:25][CH2:26][CH3:27])=[S:22])[CH2:17][CH2:18][CH3:19]>>[BrH:1].[CH2:24]([N:23]1[C:3]([C:5]2[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=2)([OH:4])[CH2:2][S:22][C:21]1=[N:20][CH2:16][CH2:17][CH2:18][CH3:19])[CH2:25][CH2:26][CH3:27]Komponenten
3
Versuchsvorschrift
6.2 g of 2 bromo-4'-chloro-3'-sulfamoylacetophenone were reacted with 3.8 g of 1,3-di-n-butylthiourea according to the prescription given in Example 12 and the end product was precipitated with diisopropyl ether.
Aufarbeitung
- customthe end product was precipitated with diisopropyl ether