N,N'-Dibutylthiourea → 3-n-Butyl-2-n-butylimino-4-(4-chloro-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrochloride

HRID 461118

Reaktionsgleichung

Reaktionsgleichung von HRID 461118
[Cl:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=1)=[O:4].[CH2:16]([NH:20][C:21]([NH:23][CH2:24][CH2:25][CH2:26][CH3:27])=[S:22])[CH2:17][CH2:18][CH3:19]>>[ClH:1].[CH2:24]([N:23]1[C:3]([C:5]2[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=2)([OH:4])[CH2:2][S:22][C:21]1=[N:20][CH2:16][CH2:17][CH2:18][CH3:19])[CH2:25][CH2:26][CH3:27]

Komponenten

3

Edukt 2

HCID 2723622N,N'-DibutylthioureaHCID 21316749HCID 21316749, Verbindung

Produkt 1

HCID 227606883-n-Butyl-2-n-butylimino-4-(4-chloro-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrochloride

Versuchsvorschrift

5.2 g of 2,4'-dichloro-3'-sulfamoylacetophenone were reacted with 3.8 g of 1,3-di-n-butylthiourea according to the prescription given in Example 12 and the end product was precipitated with diisopropyl ether.

Aufarbeitung

  1. customthe end product was precipitated with diisopropyl ether

Quellen und Nachweise

ORD-Eintrag
ord-58ff00f1d9ae47068b247a3bdca91b65
Quelldatensatz
uspto-grants-1977_12
Patentnummer
US04061761

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