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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 461156Erstellt: 26. Oktober 2026

N,N'-Diethylthiourea → 3-Ethyl-2-ethylimino-4-(4-methyl-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrochloride

https://huagongshe.com/reaction/461156

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktN,N'-DiethylthioureaHCID 2735009—
Edukt2-Chloro-4'-methyl-3'-sulfamoylacetophenoneHCID 13628783—
LösungsmittelDiisopropyl EtherHCID 7914—
Produkt3-Ethyl-2-ethylimino-4-(4-methyl-3-sulfamoylphenyl)-1,3-thiazolidine-4-ol-hydrochlorideHCID 22760433—

Reaktionsschritte

5 g of 2-chloro-4'-methyl-3'-sulfamoylacetophenone and 2.7 g of 1,3-diethylthiourea were reacted as prescribed in Example 12. After addition of 200 ml of diisopropyl ether the solvent was decanted and the oily end product was crystallized under ethyl acetate heated to 40° to 50° C. Colorless solid body, melting point: 160° C (decomposition).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04061761
Quelldatensatzuspto-grants-1977_12
ORD IDord-31fcc2290c774320bcc607a62f00ec11
Quellennotizuspto-grants-1977_12