2-Chloro-4'-methyl-3'-sulfamoylacetophenone → HCID 22760554, Verbindung

HRID 461157

Reaktionsgleichung

Reaktionsgleichung von HRID 461157
[Cl:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([CH3:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=1)=[O:4].[N:16]1[CH2:21][CH2:20][CH2:19][NH:18][C:17]=1[SH:22]>>[ClH:1].[OH:4][C:3]1([C:5]2[CH:10]=[CH:9][C:8]([CH3:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=2)[N:18]2[CH2:19][CH2:20][CH2:21][N:16]=[C:17]2[S:22][CH2:2]1

Komponenten

3

Edukt 2

HCID 136287832-Chloro-4'-methyl-3'-sulfamoylacetophenoneHCID 178527864HCID 178527864, Verbindung

Produkt 1

HCID 22760554HCID 22760554, Verbindung

Versuchsvorschrift

5 g of 2-chloro-4'-methyl-3'-sulfamoylacetophenone and 2.35 g of ground 3,4,5,6-tetrahydro-2-pyrimidine-thiol were reacted as prescribed in Example 12 and worked up as prescribed in Example 67d). Colorless crystals, melting point: 190° C (decomposition).

Quellen und Nachweise

ORD-Eintrag
ord-adfeee94392d456dabdd82142130dbdc
Quelldatensatz
uspto-grants-1977_12
Patentnummer
US04061761

Verknüpfte Notizen

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