HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Diazomethane → 3'-Sulfamoyl-diazoacetophenone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Diazomethane | HCID 9550 | — |
| Edukt | 3-Sulfamoylbenzoyl chloride | HCID 18801883 | — |
| Lösungsmittel | Diethyl Ether | HCID 3283 | — |
| Produkt | 3'-Sulfamoyl-diazoacetophenone | HCID 53705814 | — |
Reaktionsschritte
11 g of 3-sulfamoylbenzoyl chloride were reacted as prescribed in Example 66b) with diazomethane in diethyl ether and the crystals were filtered off. Melting point: 142° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04061761 |
| Quelldatensatz | uspto-grants-1977_12 |
| ORD ID | ord-29a7aeba45ad449fbac66113ff177cd3 |
| Quellennotiz | uspto-grants-1977_12 |