Methyl Bromide → Methyl dicyclohexylphosphinodithioate

HRID 461610

Reaktionsgleichung

Reaktionsgleichung von HRID 461610
[CH3:1]Br.[CH:3]1([P:9]([CH:12]2[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]2)([SH:11])=[S:10])[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1>>[CH:3]1([P:9]([CH:12]2[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]2)([S:11][CH3:1])=[S:10])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]1

Komponenten

3

Edukt 2

HCID 6323Methyl BromideHCID 75641Phosphinodithioic acid, dicyclohexyl-

Produkt 1

HCID 21391613Methyl dicyclohexylphosphinodithioate

Versuchsvorschrift

Methyl bromide was reacted with the ammonium salt of dicyclohexylphosphinodithioic acid to obtain methyl dicyclohexylphosphinodithioate, m.p. 75°-75.5° C, which on testing lasted 1500 hours* longer than the control. The average total number of hours required to each failure was 3.4 times that of the control.

Quellen und Nachweise

ORD-Eintrag
ord-5d5281a8850b4eb1a7f44b2933f67457
Quelldatensatz
uspto-grants-1977_12
Patentnummer
US04064106

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