HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4,5-Dichloro-2-nitroaniline → 11,12-Dichlorodibenzo(a,c)phenazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4,5-Dichloro-2-nitroaniline | HCID 81149 | — |
| Edukt | 1,2-Phenanthrenedione | HCID 3080566 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | 11,12-Dichlorodibenzo(a,c)phenazine | HCID 21391726 | 99,9% |
Reaktionsschritte
When 0.14 mole each of 3,4-dichloro-6-nitroaniline and phenanthrenequinone were reacted by the method of Example 1, 48.8 g. (99.9 percent yield) of 11,12-dichlorodibenzo[a,c]phenazine, mp = 263°-264° C. (DMF), were obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04064127 |
| Quelldatensatz | uspto-grants-1977_12 |
| ORD ID | ord-1f5e985d9ba34c568208de86f6e89620 |
| Quellennotiz | uspto-grants-1977_12 |