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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 461697Erstellt: 24. Oktober 2026

Benzoyl Peroxide → Methyl 2-(1-bromoethyl)benzoate

https://huagongshe.com/de/reaction/461697

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBenzoyl PeroxideHCID 7187—
EduktN-bromobutanimideHCID 67184—
EduktMethyl 2-ethylbenzoateHCID 583295—
LösungsmittelCarbon TetrachlorideHCID 5943—
ProduktMethyl 2-(1-bromoethyl)benzoateHCID 15870654—

Reaktionsschritte

A mixture of 10.7 g. (0.065 mole) of methyl 2-ethylbenzoate, 12.5 g. (0.07 mole) of N-bromosuccinimide, 50 mg. of benzoyl peroxide, and 125 ml. of carbon tetrachloride is stirred at reflux until the reaction is complete in 2 hours. The precipitated succinimide is filtered from the cooled mixture and the filtrate is evaporated to dryness under reduced pressure leaving methyl 2-(1-bromoethyl)benzoate as the residual yellow oil in quantitative yield.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04064139
Quelldatensatzuspto-grants-1977_12
ORD IDord-9f80e3ccfa154d83ac3dbd8a07af416a
Quellennotizuspto-grants-1977_12