HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-(3-(dimethylamino)propyl)formamide → N,N-dimethyl-N-(4-nitrophenyl)carbamylmethyl-N-3-formamidopropylammonium chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-(3-(dimethylamino)propyl)formamide | HCID 80020 | — |
| Edukt | Acetanilide, 2-chloro-4'-nitro- | HCID 140220 | — |
| Lösungsmittel | Isopropanol | HCID 3776 | — |
| Produkt | N,N-dimethyl-N-(4-nitrophenyl)carbamylmethyl-N-3-formamidopropylammonium chloride | HCID 86733006 | — |
Reaktionsschritte
In a manner similar to that described above in 1a, and using 14.2 parts of N-(3-dimethylaminopropyl)formamide, 20.0 parts of 2-chloro-4'-nitroacetanilide, and 78 parts of isopropyl alcohol there was obtained 27.4 parts of N,N-dimethyl-N-(4-nitrophenyl)carbamylmethyl-N-3-formamidopropylammonium chloride as a white solid which melted at 195°-196° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04065500 |
| Quelldatensatz | uspto-grants-1977_12 |
| ORD ID | ord-402c1ace94fc4ca599dadaf99a086bcf |
| Quellennotiz | uspto-grants-1977_12 |