HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-(3-(dimethylamino)propyl)formamide → N,N-dimethyl-N-(5-nitro-2-methoxyphenyl)carbamylmethyl-N-3-formamidopropylammonium chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-(3-(dimethylamino)propyl)formamide | HCID 80020 | — |
| Edukt | 2-chloro-N-(2-methoxy-5-nitrophenyl)acetamide | HCID 2362603 | — |
| Lösungsmittel | Isopropanol | HCID 3776 | — |
| Produkt | N,N-dimethyl-N-(5-nitro-2-methoxyphenyl)carbamylmethyl-N-3-formamidopropylammonium chloride | HCID 86733013 | — |
Reaktionsschritte
In a manner similar to that described above in B-1a, and using 27.3 parts of N-(3-dimethylaminopropyl)formamide, 48 parts of 2-chloro-2'-methoxy-5'-nitroacetanilide, and 157 parts of isopropyl alcohol there was obtained 52.6 parts of N,N-dimethyl-N-(5-nitro-2-methoxyphenyl)carbamylmethyl-N-3-formamidopropylammonium chloride as a white solid, m.p. 86°-88°.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04065500 |
| Quelldatensatz | uspto-grants-1977_12 |
| ORD ID | ord-be147f3e19b641a9837d46e8cfee54c9 |
| Quellennotiz | uspto-grants-1977_12 |