HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Isatoic Anhydride → N-ethylisatoic anhydride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Isatoic Anhydride | HCID 8359 | — |
| Edukt | Sodium hydride ethyl bromide | HCID 131714203 | — |
| Produkt | N-ethylisatoic anhydride | HCID 3249856 | 61% |
Reaktionsschritte
From Hardtmann et al., Journal of Heterocyclic Chemistry, Vol. 12, p. 565 (1975), it is known that isatoic anhydride can be alkylated with a sodium hydride/ethyl bromide system to provide a 61% yield of N-ethyl isatoic anhydride after recrystallization.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04515945 |
| Quelldatensatz | uspto-grants-1985_05 |
| ORD ID | ord-4590a7fde92a435fa600b2124f822c14 |
| Quellennotiz | uspto-grants-1985_05 |