HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Ethylhexylamine → HCID 178438302, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Ethylhexylamine | HCID 7719 | — |
| Edukt | Allylbicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic anhydride | HCID 54206110 | — |
| Produkt | HCID 178438302 | HCID 178438302 | — |
Reaktionsschritte
The procedure described in Example 3 is repeated, except that 204 g of allyl-bicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid anhydride and 129 g of 2-ethylhexylamine are used. 17 g of water are split off at 115° to 160° C. under 4,000 Pa in the course of 4.5 hours. 292.05 g (92.6% of theory) of a fraction of boiling point 160°-164° C. under 10.7 Pa, nD20 1.5038 and η25 0.68 Pa.s are obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04515962 |
| Quelldatensatz | uspto-grants-1985_05 |
| ORD ID | ord-66646a12f77d4dda98649accf3d14af1 |
| Quellennotiz | uspto-grants-1985_05 |