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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 462820Erstellt: 24. Oktober 2026

Chlorine → Pyridine, 2,3,4,5-tetrachloro-6-(trichloromethyl)-

https://huagongshe.com/de/reaction/462820

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktChlorineHCID 24526—
EduktPyridine, 3,4,5-trichloro-2-(trichloromethyl)-HCID 70990—
ProduktPyridine, 2,3,4,5-tetrachloro-6-(trichloromethyl)-HCID 7081165%

Reaktionsschritte

Summarizing Example 1, starting with fifty grams of a mixture rich in 3,4,5-trichloro-2-trichloromethyl pyridine, the analysis of which is set forth in Table One, and which contained 3% by weight ferric chloride, its chlorination with 70 grams per hour of chlorine, sparged into a 250 ml glass reactor at 200° C. for 5 hours, resulted in a product the analysis of which is set forth in Table One. As will be noted, a molar yield in excess of 65% of 3,4,5,6-tetrachloro-2-trichloromethyl pyridine based on 3,4,5-trichloro-2-trichloromethyl pyridine conversion was obtained.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04517369
Quelldatensatzuspto-grants-1985_05
ORD IDord-15312b5ae56c4930b6453021c4f264c6
Quellennotizuspto-grants-1985_05