Thionyl Chloride → HCID 178444542, Verbindung

HRID 462875

Reaktionsgleichung

Reaktionsgleichung von HRID 462875
[CH2:1]([C@H:6]1[CH2:11][CH2:10][C@H:9]([C:12]([OH:14])=O)[CH2:8][CH2:7]1)[CH2:2][CH2:3][CH2:4][CH3:5].S(Cl)([Cl:17])=O>>[CH2:1]([C@H:6]1[CH2:11][CH2:10][C@H:9]([C:12]([Cl:17])=[O:14])[CH2:8][CH2:7]1)[CH2:2][CH2:3][CH2:4][CH3:5]

Komponenten

3

Edukt 2

HCID 24386Thionyl ChlorideHCID 178444557HCID 178444557, Verbindung

Produkt 1

HCID 178444542HCID 178444542, Verbindung

Versuchsvorschrift

5.58 g Of trans-4-pentylcyclohexylcarboxylic acid was heated with 20 ml of thionyl chloride under reflux conditions. After the reaction was completed, the excess of thionyl chloride was removed completely under reduced pressure and the product residue obtained was distilled under reduced pressure. Trans-4-pentylcyclohexylcarbonyl chloride having a boiling point of 103° to 105° C./0.5 mmHg was obtained.

Aufarbeitung

  1. customthe excess of thionyl chloride was removed completely under reduced pressure
  2. customthe product residue obtained
  3. distillationwas distilled under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-a6066b6dbaaa4fe79ddd37f85dbd565e
Quelldatensatz
uspto-grants-1985_05
Patentnummer
US04518226

Verknüpfte Notizen

Wird geladen…