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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 463539Erstellt: 23. Oktober 2026

2-Propanol, 1,3-dichloro-, 2-carbamate → 1,3-dichloropropan-2-yl carbamate;ditridecyl (Z)-but-2-enedioate

https://huagongshe.com/de/reaction/463539

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2-Propanol, 1,3-dichloro-, 2-carbamateHCID 68516—
Edukt1,1-Bis(tert-butylperoxy)cyclohexaneHCID 76359—
Edukt2-Butenedioic acid (2Z)-, 1,4-ditridecyl esterHCID 6437427—
Produkt1,3-dichloropropan-2-yl carbamate;ditridecyl (Z)-but-2-enedioateHCID 131712900—

Reaktionsbedingungen

Temperatur110 °C

Reaktionsschritte

To a 500 ml resin kettle equipped with an overhead stirrer and containing 200 g of Flo Mo 36 C (ethoxylated castor oil) were added 50 g ditridecyl maleate and 6 g 1,1-bis(t-butylperoxy)cyclohexane (available from Witco Chemical Company under the tradename USP-400P). The mixture was then heated to 110° C. for 4 hours under nitrogen to yield a viscous liquid surfactant of the invention (Surfactant No. 54).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04520140
Quelldatensatzuspto-grants-1985_05
ORD IDord-3414ce7107c148798ef167c89ac2f26c
Quellennotizuspto-grants-1985_05